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2003 FALL MEETING PROCEEDINGS

Symposium U
Thin Films--Stresses and Mechanical Properties X

Editors: Sean G. Corcoran, Young-Chang Joo, Neville R. Moody, Zhigang Suo

MRS Proceedings Volume 795
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Mechanical Strain Evolution in Cu/low K Interconnect Lines U1.1
Paul R. Besser and Qing-Ting Jiang

Irreversible Tensile Stress Development in PECVD Silicon Nitride Films U1.6
Michael P. Hughey and Robert F. Cook

X-ray Microbeam Diffraction Measurements in Polycrystalline Aluminum and Copper Thin Films U1.7
L.E. Moyer, G.S. Cargill III, W. Yang, B.C. Larson, and G.E. Ice

Use of the Curvature Method to Determine the Misfit Stress of Epitaxial Semiconducting Systems: The Case of Samples Thinned for TEM Observation U1.9
A. Ponchet, M. Cabié, L. Durand, M. Rivoal, and A. Rocher

Dislocation Image Stresses at Free Surfaces by the Finite Element Method U2.4
Meijie Tang, Guanshui Xu, Wei Cai, and Vasily Bulatov

Phase Field Modeling of Surface Instabilities Induced by Stresses U2.10
D.J. Seol, S.Y. Hu, Z.K. Liu, S.G. Kim, W.T. Kim, K.H. Oh, and L.Q. Chen

Fracture in Thin Oxide Films U3.1
D.F. Bahr, A.L. Olson, K.R. Morasch, M.S. Kennedy, D. Rodriguez Marek, and A. Alamr

Measurement of Residual Stress in ZnO Thin Films Deposited on Silicon Wafers by the Indentation Fracture Test U3.3
Tong-Yi Zhang and Bin Huang

Thin Film Herringbone Buckling Patterns U3.4
Xi Chen and John W. Hutchinson

The Effect of Oxygen on Adhesion of Thin Copper Films to Silicon Nitride U3.6
Mengzhi Pang, Monika Backhaus-Ricoult, and Shefford P. Baker

Fracture Patterns in Thin Films and Multilayers U3.8
Alex A. Volinsky, Dirk C. Meyer, Tilmann Leisegang, and Peter Paufler

Toughness and Contact Behavior of Conventional and Low-k Dielectric Thin Films U4.1
Robert F. Cook, Dylan J. Morris, and Jeremy Thurn

Understanding Adhesion Failure in Low-k Dielectric Stack During Chemical-Mechanical Polishing U4.3
F. Iacopi, D. Degryse, I. Vos, M. Patz, and K.Maex

Solutions and Discussions of Thin Film Undergoing the Nonlinear Peeling U4.5
Yueguang Wei, Siqi Shu, and Ying Du

Effects of Varying Mean Stress and Stress Amplitude on the Fatigue of Polysilicon U4.7
H. Kahn, R. Ballarini, and A.H. Heuer

Fracture Behavior of Micro-Sized Specimens Prepared from a TiAl Thin Foil U4.9
K. Takashima, T.P. Halford, D. Rudinal, Y. Higo, and P. Bowen

A Membrane Deflection Fracture Experiment to Investigate Fracture Toughness of Freestanding MEMS Materials U4.10
H.D. Espinosa and B. Peng

Stress Relaxation During Isothermal Annealing at Elevated Temperatures in Electroplated Cu Films U5.1
Soo-Jung Hwang, Young-Chang Joo, and Junichi Koike

Stress and Texture in Sputter Deposited Cr Films U5.5
S. Yu. Grachev, J.-D. Kamminga, and G.C.A.M. Janssen

Thickness Dependent Stress Relaxation With the Onset of L10 Ordering in FePt Thin Films U5.8
K.W. Wierman, C.L. Platt, and J.K. Howard

Single-Crystal and Nano-Columnar Growth of Gadolinium-Doped Ceria Thin Films on Oxide Substrates Studied Using Electron Microscopy U5.9
D.X. Huang, C.L. Chen, and A.J. Jacobson

Strain Control in SrRuO3 Thin Films by Using a Lattice Constant Tunable Buffer U5.10
K. Terai, T. Ohnishi, M. Lippmaa, H
. Koinuma, and M. Kawasaki

Thermal Stability and Internal Stress for Strongly (111) Oriented Cu Films U5.11
Sinji Takayama , Makato Oikawa, and Tokuji Himuro

Stress and Defect Generation in Si Epitaxy U5.12
Tien Wang and Douglas Carlson

Interdiffusion in Coherent Si0.90Ge0.10/Si0.95Ge0.05 Superlattices U5.14
D.B. Aubertine and P.C. McIntyre

Evaluation on Stress and Optical Property of Thin Films Used in Optical MEMS Device U5.17
Lianchao Sun and Ping Hou

In Situ Investigation of Growth of Gold on Crystalline TiO2 and Amorphous Al2O3 Substrates U5.18
L. Lauter and R. Abermann

Formability of Ultra-Thin Plasma-Polymer Films Deposited on Metal Sheet: Mesoscopic and Nanoscopic Aspects of Defect Formation U5.23
B. Baumert, M. Stratmann, and M. Rohwerder

Investigation of Mechanical Properties of Mesoporous Methyl-Substituted SiO2 Thin Films (Methylsilesquioxane Materials) U5.26
M. Verdier, M. Montagnat, S. Maîtrejean, and G. Passemard

In Situ, Real-Time Curvature Imaging During Chemical Vapor Deposition U5.31
David A. Boyd, Ashok B. Tripathi, Mohamed El-Naggar, and David G. Goodwin

Effect of Dielectric Materials on Stress-Induced Damage Modes in Damascene Cu Lines U6.2
Jong-Min Paik, Hyun Park, Ki-Chul Park, and Young-Chang Joo

Young's Modulus Variation with Thickness of Thin Films U6.6
L.G. Zhou and Hanchen Huang

Stretchable Conductors: Thin Gold Films on Silicone Elastomer U6.9
Stéphanie P. Lacour, Sigurd Wagner, and Z. Suo

Stress-Assisted Copper-induced Lateral Growth of Polycrystalline Germanium U6.10
B. Hekmatshoar, D. Shahrjerdi, S. Mohajerzadeh , A. Khakifirooz, M. Robertson, and A. Afzali-Kusha

Probing Strain Fields About Thin Film Structures Using X-Ray Microdiffraction U7.3
C.E. Murray, I.C. Noyan, P.M. Mooney, B. Lai, and Z. Cai

Effects of the Substrate on the Determination of Hardness of Thin Films by the Nanoscratch and Nanoindentation Techniques: A Comparative Study for the Cases of Soft Film on Hard Substrate and Hard Film on Soft Substrate U7.5
Noureddine Tayebi, Andreas A. Polycarpou, and Thomas F. Conry

Dislocation Nucleation and Segregation in Nano-scale Contact of Stepped Surfaces U7.9
H.H. Yu, P. Shrotriya, J. Wang, and K.-S. Kim

Determination of Residual-Stress-Free State and Mapping of Residual Stress Fields Using Speckle Interferometry and Thermal Relaxation U7.10
Dong-Won Kim, Jong-jin Kim, Dongil Son, Nak-Kyu Lee, Kyung-Hoan Na, and Dongil Kwon

Subcritical Delamination of Dielectric and Metal Films from Low-k Organosilicate Glass (OSG) Thin Films in Buffered pH Solutions U8.1
Y. Lin, J.J. Vlassak, T.Y. Tsui, and A.J. McKerrow

Bonding Characterization of Oxidized PDMS Thin Films U8.3
J.J. McMahon, Y. Kwon, J.-Q. Lu, T.S. Cale, and R.J. Gutmann

Effects of Process Parameters on the Adhesion of Copper Film on Polyethylene Tetrephthalate(Pet) Substrate Prepared by ECRMOCVD Coupled with a Periodic DC Bias U8.5
Jin Hyun, Bup Ju Jeon, Dongjin Byun , and Joong Kee Lee

Adhesion Strength of Polymer Coatings Studied by Laser Induced Delamination U8.6
A. Fedorov, A. van Veen, R. van Tijum, and J.Th.M. de Hosson

An Atomistic View of Interface-Mediated Dislocation Plasticity in Thin Metal Films U8.8
E.S. Ege and Y.-L. Shen

Dislocation Dynamics in Semiconductor Thin Film-Substrate Systems U8.9
E.H. Tan and L.Z. Sun

Microstructural Aspects of Fracture in Nanolayered TiAlCrN Thin Films U8.10
A. E. Santana, A. Karimi, V.H. Derflinger, and A. Schütze

Internal Oxidation and Mechanical Properties of Pt-IrO2 Thin Films U8.13
Richard R. Chromik, Thirumalesh Bannuru, and Richard P. Vinci

Cracking and Phase Transformation in Silicon During Nanoindentation U8.15
Jae-il Jang, Songqing Wen, M.J. Lance, I.M. Anderson, and G.M. Pharr

Scratch Test Measurements on CrNx Coatings U8.16
R. Hoy, P. van Essen, J.-D. Kamminga, G.C.A.M. Janssen, A.P. Ehiasarian

Resistance to Cracking of a Stretchable Semiconductor: Speed of Crack Propagation for Varying Energy Release Rate U8.19
Sheng Liu, Hee C. Lim, Min Qu, John F. Federici, Gordon A. Thomas, Helena Gleskova, and Sigurd Wagner

Microstructure Evolution of On-Substrate NiTi Shape Memory Alloy Thin Films U8.20
Xi Wang, Ann Lai, Joost J. Vlassak, and Yves Bellouard

Mechanisms Controlling the Hardness of Si and Ge U8.22
L.J. Vandeperre, F. Giuliani, S.J. Lloyd, and W.J. Clegg

Computational and Experimental Characterization of Indentation Creep U8.23
Ming Dao, Hidenari Takagi, Masami Fujiwara, and Masahisa Otsuka

Tuning the Mechanical Properties of SiO2 Thin Film for MEMS Application U8.25
Wang-Shen Su, Weileun Fang, and Ming-Shih Tsai

Optimization of Film Stresses Utilized in Composite Piezoelectric Membrane Microgenerators U8.26
M.S. Kennedy, M. Zosel, C.D. Richards, R.F. Richards, D.F. Bahr, K.W. Hipps, and N.R. Moody

Stress and Strength of Free-Standing 2-Dimensional Tetrahedral Amorphous Carbon Bridge Arrays U8.27
Daniel H.C. Chua, T.H. Tsai W.I. Milne, D. Sheeja, and B.K. Tay

Nanoindentation Behavior of Gold Single Crystals U8.30
Martha M. McCann and Sean G.Corcoran

Determination of Mechanical Parameters for Rotating MEMS Structures as a Function of Deposition Method U9.2
S. Soare, S.J. Bull, A. Oila, A.G. O'Neill, N. Wright, A. Horsfall, and J. dos Santos

Direct Observations of Grain Boundary Phenomena During Indentation of Al and Al-Mg Thin Films U9.3
W.A. Soer, J.Th.M. De Hosson, A.M. Minor, E.A. Stach, and J.W. Morris Jr.

Experimental Measurements of Surface Residual Stress Caused by Nano-scale Contact of Rough Surfaces U9.9
J. Wang, P. Shrotriya, H.H. Yu, and K.-S. Kim

Bulge Test on Free Standing Gold Thin Films U10.3
Yawen Li and Michael J. Cima

Microstructure–Mechanical Properties Relationship of Laser Interference Irradiated Ni/Al Multi-Film U10.4
C. Daniel, A. Lasagni, and F. Mücklich

Early Yielding and Stress Recovery in (111) and (100) Texture Components in Cu Thin Films Determined Using Synchrotron X-ray Diffraction U10.5
D.E. Nowak and S.P. Baker

Indentation and Finite Element Modeling Investigations of the Indentation Size Effect in Aluminium Coatings on Borosilicate Glass Substrates U10.6
I. Spary, N. M.Jennett, and A.J. Bushby

Young's Modulus, Poisson's Ratio, and Nanoscale Deformation Fields of MEMS Materials U10.9
I. Chasiotis, S.W. Cho, T.A. Friedmann, and J.P. Sullivan

Hinge Sensitivity in a Micro-Rotating Structure for predicting Induced Thermo Mechanical Stress in Integrated Circuit Metal Interconnects U10.10
J.M.M. dos Santos, K. Wang, S.M. Soare, S.J. Bull, A.B. Horsfall, N.G. Wright, A.G. O'Neill, J.G. Terry, A.J. Walton, A.M. Gundlach, and J.T.M. Stevenson

Modeling and Optimal Design of Multilayer Cantilever Microactuators U10.11
L.H. Han and T.J. Lu

Mechanical Properties and Morphology of Polycrystalline 3C-SiC Films Deposited on Si and SiO2 by LPCVD U11.3
Xiao-an Fu, Jeremy Dunning, Srihari Rajgopal, and Ming Zhang

Residual Stress in Silicon Nitride Thin Films Deposited by ECR-PECVD U11.4
E. Cianci and V. Foglietti

A Study on Selective Etching of SiGe Layers in SiGe/Si Systems for Device Applications U11.8
Takashi Yamazaki, Tomohide Sekikawa, Shinya Morita, Yoshitaka Hakamada, Hiroyuki Ohri, Shun-ichiro Ohmi, and Tetsushi Sakai

Guided Formation of Nanostructures in Thin Films U11.10
Wei Lu and Dongchoul Kim

Indentation Curve Analysis for Pile-up, Sink-In and Tip-Blunting Effects in Sharp Indentations U11.13
Yeol Choi, Baik-Woo Lee, Ho-Seung Lee, and Dongil Kwon

Determining Stress-strain Curves for Thin Films by Experimental/Computational Nanoindentation U11.14
Baik-Woo Lee, Yeol Choi, Yun-Hee Lee, Ju-Young Kim, and Dongil Kwon

A Theoretical Study on the Indentation of Viscoelastic Materials U11.16
Guanghui Fu

Effects of Thickness and Indenter Geometry in Nanoindentation of Nickel Thin Films U11.19
Padma Parakala, Reza A. Mirshams, Seifollah Nasrazadani, and Kun Lian

Thermo-Mechanical Behavior of Fe Thin Films U11.23
Nail R. Chamsoutdinov, Amarante J. Böttger, Rob Delhez, and Frans D. Tichelaar

Thermomechanical Behavior of Tantalum Thin Films: The Effects of Oxygen and the b - a Phase Transformation U11.27
Robert Knepper, Blake Stevens, and Shefford P. Baker

Thin Film Material Parameters Derived From Full Field Nanometric Displacement Measurements in Non-Uniform MEMS Geometries U11.28
Jaime F. Cárdenas-García, Sungwoo Cho, and Ioannis Chasiotis

Temperature Dependence of Biaxial Modulus and Thermal Expansion Coefficient of Thin Films Using Wafer Curvature Method U11.29
M. Capanu, A. Cervin-Lawry, A. Patel, I. Koutsaroff, P. Woo, Lynda Wu, J. Oh, J. Obeng, and B. McClelland

Characterizing Thin-Film Stress Fields by Resonance of Membrane Arrays U11.32
R. Engelstad, E. Lovell, A. Chalekian, S. Janowski , M. Cash, and H. Eguchi

Measurement of Thin-Film Stress, Stiffness, and Strength Using an Enhanced Membrane Pressure-Bulge Technique U11.34
Aaron J. Chalekian, Roxann L. Engelstad, and Edward G. Lovell

Thermal-Mechanical Evaluation of Plated Electro-Magnetic NiFe for MEMS Generators U11.35
Yibin Xue, Keithan Hillman, and David Veazie

The Effects of Passivation Layer and Film Thickness on the Mechanical Behavior of Freestanding Electroplated Cu Thin Films With Constant Microstructure U11.37
Yong Xiang, Joost J. Vlassak, Maria T. Perez-Prado, Ting Y. Tsui, and Andrew J. McKerrow

Monotonic Testing and Tension-Tension Fatigue Testing of Free-Standing Al Microtensile Beams U11.39
Nicholas Barbosa III, Paul El-Deiry, and Richard P. Vinci

The Thermal Annealing Effect on the Residual Stress and Interface Adhesion in the Compressive Stressed DLC Film U11.42
Heon Woong Choi, Myoung-Woon Moon, Tae-Young Kim, Kwang-Ryeol Lee, and Kyu Hwan Oh

Effect of Monazite Coating on Tensile Properties of Nextel 720 Fibers, Tows and Minicomposites U11.43
Devdas M. Pai, Sergey Yarmolenko, Jagannathan Sankar, Balasubramanian Kailasshankar, Christopher Murphy, Edwardo Freeman, and Larry P. Zawada

Microstructure and Current Transport Properties of YBa2Cu3O7-x/(Ba0.05, Sr0.95)TiO3 Multiple-Layer Thin Films U11.46
Y. Luo, R.A. Hughes, J.S. Preston, and G.A. Botton

Stress-Field in Sputtered Mo Thin Films and Mo/Ni Superlattices: Origin and Evolution After Ion-Irradiation U12.3
A. Debelle, G. Abadias, A. Michel, C. Jaouen, Ph. Guérin, and M. Drouet

Asymmetry in Multilayer Adhesion: the Zinc Oxide/Silver Interface U12.5
E. Barthel, P. Nael, O. Kerjan, and N. Nadaud

Design Maps for the Tensile Yield Strength of Nanoscale Metallic Multilayers U12.7
Adrienne V. Lamm and Peter M. Anderson

DLC/Hydroxyapatite Nanocomposites U12.9
Roger J. Narayan


Investigation of Structural and Mechani
cal Properties of UV and Microwave-Irradiated Al2O3/ZrO2 Multilayers by Sol-Gel Coating U12.11
A.R. Phani and H. Haefke



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